›› 2006, Vol. 1 ›› Issue (1): 20-24.

• 论文 • Previous Articles     Next Articles

Application of HSQC-TOCSY to the Analysis of Saponins

Yue Cong1*; Wen Li 2; Changda Liu 1; Jinhu Wang1; and Xian Li 1   

  1. 1. School of Traditional Chinese Materia Medica, Shenyang Pharmaceutical University, Shenyang 110016, China; 2. Center of Analysis and Test, Shenyang Pharmaceutical University, Shenyang 110016, China
  • Received:2006-01-01 Revised:2006-01-01 Online:2006-02-15 Published:2006-02-15
  • Contact: Yue Cong

Abstract: HSQC-TOCSY is a useful 2D NMR method for determining the structures of organic molecules that
possess independent spin systems. In this paper, 5 compounds have been isolated from the leaves and stems of
Panax quinquefolium L.. and they are used to demonstrate the application of this technique. The 13C and 1H
chemical shifts of the sugar moiety of the 5 compounds were assigned accurately.

Key words: HSQC-TOCSY, 2D NMR, chemical shift, saponins, leaves and stems of Panax quinquefolium L.

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